| The UCLA ims 1270 uses both the standard CAMECA Cs+ (microbeam) and
duoplasmatron primary ion sources. While either source is capable of producing ion
beams as small as 1 µm diameter, most isotopic analyses utilize beam diameters in the 10
to 30 µm range to quickly achieve desired precision. Like the SHRIMP ion probe, the
1270 routinely attains a mass resolving power (MRP) of up to 5,000 without significant
loss of secondary ion intensity; this is necessary for isotopic analysis of certain trace
elements at high sensitivity (e.g., Pb in a zircon). Dynamic mass range is 300 (H to
UO2). |

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| Like the smaller CAMECA instruments, the 1270 also
functions as an ion microscope by direct ion imaging of the sample (with ~0.5 µm lateral
resolution), which is a key component for achieving good (~nm scale) spatial resolution
during depth-profiling (because it enables elimination of crater edge
contributions). For the analysis of negative secondary ions from electrically
insulating samples (e.g., O isotope measurements in silicates or carbonates), a normal
incidence electron flood gun provides charge compensation. This is the only method
that has been demonstrated to work routinely for high-precision oxygen isotope
measurements. A five moveable collector ion detection system is operational for
several types of isotopic analyses. In some favorable cases, precision of isotopic
ratios achieved in multicollector mode is comparable to that typical of other traditional
high-precision mass spectrometric methods although with SIMS the spatial information
regarding complex isotopic distributions in a sample is preserved. The
multicollector enables new types of scientific investigations, and has been increasingly
utilized by visitors to the facility, particularly for investigations of C, O, and S
isotopes. |
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Schematic representation of the detector system and projection
optics of the UCLA ims 1270. When the full multicollector array is used, the axial
adjustable exit slit and projection lens is lifted out of the secondary ion beam path,
allowing the detector modules to be translated along the mass focal plane. The
extreme detector modules (L2 and H2) have mounted fixed Faraday cups (L2 and
H2) so that L2 and H2 are always configured with an electron multiplier (EM).
The detectors in L1, C, and H1 can be either an EM or a Faraday cup. The detector
electronics are provided by a Finnigan module (for FC) or a CAMECA-CAMAC based
pulse-counting system (for EM). |